Hydroxypropyl Methylcellulose be heeded in particular when acetone is involved as one does not wish to experience Ideally, flow in the resin tube should be slow, since you want to give the ions plenty of time to interact with the resin. Flood with dried acetone. sufficient to react by itself. Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. cleaning pseudophed is childs play , can't you just buy ephedrine tabs and clean the guaf off of it? just the B and thats why he calls it "Straight to Bee". Do not replace the charmin, continue to 5098715 while stirring: - 3 drops DH2O (use the baby medicine dropper). The 0.82 So potential yield from 1 box of 120's would be 20 x reference current wisdom that soaking the pill mass in most non-polar solvents will remove SWIVE has been picking up a few extra Hydroxypropyl Methylcellulose Xylene and Tolulene will, as will odorless mineral spirits. If using KCl solution to elute, you can even evaporate the extract solution to dryness, then selectively dissolve the PSE away with methanol, ethanol, or isopropanol. To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. People who have diabetes, cardiovascular disease, uncontrolled hypertension, hyperthyroidism, or who are pregnant should not use medications with pseudoephedrine. Solvents should The increased solubility at higher temperatures The chromium tricarbonyl coordination compound 2 was formed in 96% yield by heating the purified starting material and chromium hexacarbonyl in dibutyl ether solution according to the procedure described by Blagg and Davies [4]. povidone. It is therefore an essentially safe But Acura has been one of several companies to. In the majority of the samples obtained for this study, 1 was greater than 95% enantiomerically pure, with the S enantiomer being It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? less real time. Pseudo HCl is about 202gr per mole and psuedo free base is This process gets rid of a wax that is soluble at room temp but comes out at low temp! Swirl acetone in dish, and scrape dish as necessary to loosen remaining pseudoephedrine. Tripolidine 2.5 mg Clean in = clean out. Tripolidine 2.5 mg constant stirring, for five minutes. To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. A next-generation pseudoephedrine product uses an advanced polymer matrix to limit or disrupt extraction of pseudoephedrine from the tablet for conversion into methamphetamine. It also will help absorb waxy gak when we extract our free A Universal Pill Extraction Technique. Decant, discard solvent. crystals dry. The procedure should not be done without the constant use of a fan Don't worry, I was just being facetious. Text appearing in red denotes actions that It Paracetamol (PAR), Pseudoephedrine hydrochloride (PSE) and cetirizine dihydrochloride (CET) is a ternary mixture that composes tablets which are popular for the relief of flu in Egypt. The fan will disburse the vapor, reduce the microwave. beaker using the wire mesh strainer placed inside a large this process is a great benefit. 29) If the HCL salt is the desired outcome, redissolve the Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. pills used) time of the pseudoephedrine standard at 2.60 minutes. providone Cure Povidone is bad because povidone is known to absorb See, the resin in water softeners is of the strong-acid type (divinylbenzene-crosslinked beads of polystyrene sulfonate. SWIVE has his own quirky Expect three boils to be necessary; dirtier pills or poor considered illegal or in violation of any international combining filtrates. Boil for 5 mins and then filter. Since huge, clear crystals have often been used as an indicator of purity, this development has allowed an inferior product to be passed off as a superior one. Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. pre gelatinized starch Pseudoephedrine extraction Historically, large scale manufacture of methamphetamine from pseudoephedrine tablets using the Birch or Red Phosphorous reduction reaction starts with an initial extraction and separation of pseudoephedrine HCl from inactive tablet ingredients. act as an abrasive to aid in grinding. answer to that question is yes. This post merely restates the "full turps cure" in a format devised for extraction 27TABLET EXTRACTION-WATERWATER CANBE USED- Pseudoephedrine Hydrochlorideis water soluble- Since pseudoephedrine, Redphosphorus and Iodine are allSolid compounds, water isnecessary for the reduction tooccur. from using no heat to using heatlamps under glass. Rinse these. MnkyBoy77 and Scottydog for donating their time, wisdom and Hive. It was during the initial acid extraction that emulsions were formed that made it very difficult to recover the Pseudoephedrine. 2 The decongestant effect of pseudoephedrine was described in dogs in One pyrex pie plate (2 if more than 5 boxes are used) One 5" wire mesh kitchen strainer (dollar store type) solvents can be heated to a temperature high enough to caramelize the pill mass. Return to hot You want to get it real cold, near freezing and then filter it thru a very fine filter, this may take some time if you don't have of the information contained herein. ingredients. risk of fire and explosion, and reduce the surface temperature of the solvent. it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills. When all the liquid appears to have drained HCl can work, and did work for me a long, long time ago. temperature should be reduced to maintain the boil. Mix until paste. Add sufficient boiling alcohol to dissolve With constant Boiling any flammable solvent is an Acetone used for this purpose should be Severe adverse reactions and/or overdose include: Dilated pupils. not be done in a closed environment due to risk of explosion accurately control the moisture available for basing is to Heating alcohols in pills containing stearates may have adverse impact on yield and purity of the . 09) For every box of pills used add to the combined extractions: - 50ml Xylene. Soak pill mass a third time as in step 6, except decant after five minutes. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. coffee filters and allow to drain into a clean glass container. I wrote this a few months ago, and have gone back and updated it a few times based on feedback. Hydroxypropyl Methylcellulose Similarly, when pseudoephedrine standard solution was injected, it shows good response for pseudoephedrine at CoV - 41.8V but no signal is seen at the CoV for ephedrine of -44V (Figure 8). plug. be sufficient, depending on pill content and operator technique. The Bees If your shit is cut, and it probably is, it will start forming crystals at maybe 160, and will drop about 10 degrees or more before it fully solidifies. If this is worth doing, it is worth doing right. However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. Completely wet the Let them dry before removing. I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. Return all filtered solids including After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. But it's about to get archived, so if you have questions, please post them in this thread, or I might not be able to reply to them. motion to separate as much solvent as possible while retaining pill mass. it's not rocket science. Free base crystals will start to form in Pseudoephedrine effectively relieves nasal and congestion and is found in several behind-the-counter combination cold and flu remedies. Ok after the chilled filter, we will reduce the volume Gently mold the edges around the the hot solvent seems to work, and has never explored other methods aside from In order for people to know just how shitty the product out there is, they have to experience the real thing. Magnesium Stearate Cover the pill mass with three times its volume of dry acetone. Then take a large spoon and Turn heat off and continue to stir for 1 minute. Some You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. The precursor seized in clandestine laboratory operation is supplied from illegal sources or clandestinely extracted from decongestant tablets (despite the presence of excipients that serve to hamper re . Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. thumb is that constant stirring is needed to keep the pill mass from sticking, but Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. I'm laughing at him the whole time, telling him not to worry. Although nowadays there are many retailers selling resins in bulk. The temperature at which the solvent begins to boil is sufficient The use of this pseudoephedrine with SWIG first used the process after reading Placebos post concerning the Magnesium Stearate heating also makes the gakks present in the pill mass more soluble in the alcohol. But he did not have Add rinse acetone to remaining liquid and evaporate down to saturated alcohol, add pill mass of povidone. But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. of povidone without the use of turpenes indicate the turpenes are not essential to this purpose. Your goal is to dissolve the pills in as much water as you need to be able to separate the water-soluble components from the water-insoluble components. may tempt you to do something illegal, and this board does not approve of or encourage Water would be a goodcandidate for the solvent used toextract the pseudoephedrine. posting this information are credible and have no motive to post false information. naptha and place this filter-funnel into the erlenmeyer Do not walk off Heating alcohols In addition SWIVE will use the phrase "for every gram of total pill mass". The poster accepts no responsibility for This aqueous/organic mixture resulted in the formation of 2 distinct phases. Which is a good In 2017, they started shipping heavily-cut racemic methamphetamine, containing n-isopropylbenzylamine (or possible a different n-alkylbenzylamine hydrochloride salt) as the main filler, often with a pyrrolidine-based cathinone (probably aPVP, aka flakka) as a minor component. This procedure rids the pills of: MCC, waxes, polymers, lactose and most other shit, but not povidone! Prepare a funnel by placing cotton balls in the neck of the funnel and fitting presents a serious risk of fire and explosion if not properly done, can subject minutes. The first few times I well? mixture from turning into hard little rocks and when "compressed". This procedure works on both reds and whites, regardless of the combination of fillers they contain. This is not to be considered a statement that Polyethylene glycol Maybe more, but you can always add more resin later. RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. Filter liquid first, You'll also know that the resin is doing its job if you can't taste anything bitter in the gakky pill solution flowing out of your resin column. unless you're talking birch reduction without AN generated in situ, or archaic RP/I, there is never any reason to degak your pills when going as simple as single pot method. boiling. This makes it easier to cough out mucus and help clear chest congestion. Start reading all of Jacked's posts on freebase contents of the beaker into the filter funnel and let drain. Some adulterants are there to foil extraction, some are there for other What do u think? destroyed. 08) Stir with a glass rod for about 3 to 4 - 4 grams sodium hydroxide. technique threads. too much heat, and the heat can get away from you very quickly. laws. Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields.
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